{"id":5371,"date":"2024-04-23T16:07:42","date_gmt":"2024-04-23T08:07:42","guid":{"rendered":"https:\/\/www.51dmea.cn\/archives\/5371"},"modified":"2024-04-23T16:07:42","modified_gmt":"2024-04-23T08:07:42","slug":"nn-%e4%ba%8c%e7%94%b2%e5%9f%ba%e7%94%b2%e9%85%b0%e8%83%ba","status":"publish","type":"post","link":"https:\/\/www.51dmea.cn\/archives\/5371","title":{"rendered":"N,N-\u4e8c\u7532\u57fa\u7532\u9170\u80fa"},"content":{"rendered":"<p>    \t\t\t\t\t\t<img decoding=\"async\" loading=\"lazy\" class=\"alignnone size-full wp-image-5366\" src=\"https:\/\/www.51dmea.cn\/wp-content\/uploads\/2024\/04\/29b84359f91345d89fbd1572a8ca741a.gif\" width=\"198\" height=\"227\" alt=\"N,N-\u4e8c\u7532\u57fa\u7532\u9170\u80fa\u7ed3\u6784\u5f0f\" \/><\/p>\n<p>\u7ed3\u6784\u5f0f<\/p>\n<table class=\"summary-table table table-striped table-bordered\">\n<col width=\"90\" \/>\n<tbody>\n<tr>\n<th scope=\"row\">\u7269\u7ade\u7f16\u53f7<\/th>\n<td>01F6<\/td>\n<\/tr>\n<tr>\n<th scope=\"row\">\u5206\u5b50\u5f0f<\/th>\n<td>C3H7NO<\/td>\n<\/tr>\n<tr>\n<th scope=\"row\">\u5206\u5b50\u91cf<\/th>\n<td>73<\/td>\n<\/tr>\n<tr>\n<th scope=\"row\">\u6807\u7b7e<\/th>\n<td>\n<p>                        \u4e8c\u7532\u57fa\u7532\u9170\u80fa,<\/p>\n<p>                        \u7532\u9170\u4e8c\u7532\u80fa,<\/p>\n<p>                        \u4e8c\u7532\u66ff\u7532\u9170\u80fa,<\/p>\n<p>                        N-\u7532 \u9170\u4e8c\u7532\u80fa\uff1b,<\/p>\n<p>                        Dimethylformamide,<\/p>\n<p>                        Dormyl dimethylamine,<\/p>\n<p>                        DMF,<\/p>\n<p>                        DMFA,<\/p>\n<p>                        N-Formyldimethylamine,<\/p>\n<p>                        \u8102\u80aa\u65cf\u542b\u6c2e\u5316\u5408\u7269<\/p>\n<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<ul class=\"nav nav-tabs\">\n<li class=\"active\"><a href=\"#bh\">\u7f16\u53f7\u7cfb\u7edf<\/a><\/li>\n<li><a href=\"#wx\">\u7269\u6027\u6570\u636e<\/a><\/li>\n<li><a href=\"#dl\">\u6bd2\u7406\u5b66\u6570\u636e<\/a><\/li>\n<li><a href=\"#st\">\u751f\u6001\u5b66\u6570\u636e<\/a><\/li>\n<li><a href=\"#fz\">\u5206\u5b50\u7ed3\u6784\u6570\u636e<\/a><\/li>\n<li><a href=\"#js\">\u8ba1\u7b97\u5316\u5b66\u6570\u636e<\/a><\/li>\n<li class=\"dropdown pull-right\">\n                    <a href=\"\" class=\"dropdown-toggle\" data-toggle=\"dropdown\">\u66f4\u591a <span class=\"caret\"><\/span><\/a><\/p>\n<ul class=\"dropdown-menu\" role=\"menu\">\n<li><a href=\"#xz\">\u6027\u8d28\u4e0e\u7a33\u5b9a\u6027<\/a><\/li>\n<li><a href=\"#zc\">\u8d2e\u5b58\u65b9\u6cd5<\/a><\/li>\n<li><a href=\"#hc\">\u5408\u6210\u65b9\u6cd5<\/a><\/li>\n<li><a href=\"#yt\">\u7528\u9014<\/a><\/li>\n<\/ul>\n<\/li>\n<\/ul>\n<h2 id=\"bh\">\u7f16\u53f7\u7cfb\u7edf<\/h2>\n<p><b>CAS\u53f7\uff1a<\/b>68-12-2<\/p>\n<p><b>MDL\u53f7\uff1a<\/b>MFCD00003284<\/p>\n<p><b>EINECS\u53f7\uff1a<\/b>200-679-5<\/p>\n<p><b>RTECS\u53f7\uff1a<\/b>LQ2100000<\/p>\n<p><b>BRN\u53f7\uff1a<\/b>605365<\/p>\n<p><b>PubChem\u53f7\uff1a<\/b>24893883<\/p>\n<h2 id=\"wx\">\u7269\u6027\u6570\u636e<\/h2>\n<p><p>1.\u6027\u72b6\uff1a\u65e0\u8272\u900f\u660e\u6216\u6de1\u9ec4\u8272\u6db2\u4f53\uff0c\u6709\u9c7c\u8165\u5473\u3002<sup>[1]<\/sup><\/p>\n<p>2.\u7194\u70b9\uff08\u2103\uff09\uff1a-61<sup>[2]<\/sup><\/p>\n<p>3.\u6cb8\u70b9\uff08\u2103\uff09\uff1a153<sup>[3]<\/sup><\/p>\n<p>4.\u76f8\u5bf9\u5bc6\u5ea6\uff08\u6c34=1\uff09\uff1a0.95<sup>[4]<\/sup><\/p>\n<p>5.\u76f8\u5bf9\u84b8\u6c14\u5bc6\u5ea6\uff08\u7a7a\u6c14=1\uff09\uff1a2.51<sup>[5]<\/sup><\/p>\n<p>6.\u9971\u548c\u84b8\u6c14\u538b\uff08kPa\uff09\uff1a0.5\uff0825\u2103\uff09<sup>[6]<\/sup><\/p>\n<p>7.\u71c3\u70e7\u70ed\uff08kJ\/mol\uff09\uff1a-1921<sup>[7]<\/sup><\/p>\n<p>8.\u4e34\u754c\u6e29\u5ea6\uff08\u2103\uff09\uff1a374<sup>[8]<\/sup><\/p>\n<p>9.\u4e34\u754c\u538b\u529b\uff08MPa\uff09\uff1a4.48<sup>[9]<\/sup><\/p>\n<p>10.\u8f9b\u9187\/\u6c34\u5206\u914d\u7cfb\u6570\uff1a-0.87<sup>[10]<\/sup><\/p>\n<p>11.\u95ea\u70b9\uff08\u2103\uff09\uff1a58\uff08OC\uff09<sup>[11]<\/sup><\/p>\n<p>12.\u5f15\u71c3\u6e29\u5ea6\uff08\u2103\uff09\uff1a445<sup>[12]<\/sup><\/p>\n<p>13.\u7206\u70b8\u4e0a\u9650\uff08%\uff09\uff1a15.2<sup>[13]<\/sup><\/p>\n<p>14.\u7206\u70b8\u4e0b\u9650\uff08%\uff09\uff1a2.2<sup>[14]<\/sup><\/p>\n<p>15.\u6eb6\u89e3\u6027\uff1a\u4e0e\u6c34\u6df7\u6eb6\uff0c\u53ef\u6df7\u6eb6\u4e8e\u591a\u6570\u6709\u673a\u6eb6\u5242\u3002<sup>[15]<\/sup><\/p>\n<p>16.\u6298\u5c04\u7387\uff0825\u00baC\uff09\uff1a1.42817<\/p>\n<p>17.\u9ecf\u5ea6\uff08mPa\u00b7s,25\u00baC\uff09\uff1a0.802<\/p>\n<p>18.\u6bd4\u65cb\u5149\u5ea6\uff08\u00ba\uff09\uff1a0.94<\/p>\n<p>19.\u71c3\u70b9\uff08\u00baC\uff09\uff1a445<\/p>\n<p>20.\u84b8\u53d1\u70ed\uff08KJ\/mol,25\u00baC\uff09\uff1a47.545<\/p>\n<p>21.\u84b8\u53d1\u70ed\uff08KJ\/mol,100\u00baC\uff09\uff1a43.585<\/p>\n<p>22.\u84b8\u53d1\u70ed\uff08KJ\/mol,b.p.\uff09\uff1a38.368<\/p>\n<p>23.\u7194\u5316\u70ed\uff08KJ\/mol\uff09\uff1a16.165<\/p>\n<p>24.\u71c3\u70e7\u70ed\uff08KJ\/mol\uff09\uff1a1915.46<\/p>\n<p>25.\u6bd4\u70ed\u5bb9\uff08KJ\/(kg\u00b7K),25\u00baC,\u5b9a\u538b\uff09\uff1a2.14<\/p>\n<p>26.\u7535\u5bfc\u7387\uff08S\/m\uff09\uff1a6\u00d710<sup>-8<\/sup><\/p>\n<p>27.\u70ed\u5bfc\u7387\uff08W\/(m\u00b7K),20\u00baC\uff09\uff1a0.16579<\/p>\n<\/p>\n<h2 id=\"dl\">\u6bd2\u7406\u5b66\u6570\u636e<\/h2>\n<p><p><strong>1.\u6025\u6027\u6bd2\u6027<sup>[16]<\/sup><\/strong><\/p>\n<p>LD50\uff1a4000mg\/kg\uff08\u5927\u9f20\u7ecf\u53e3\uff09\uff1b4720mg\/kg\uff08\u5154\u7ecf\u76ae\uff09<\/p>\n<p>LC50\uff1a9400mg\/m<sup>3<\/sup>\uff08\u5c0f\u9f20\u5438\u5165\uff0c2h\uff09<\/p>\n<p><strong>2.\u523a\u6fc0\u6027<sup>[17]<\/sup><\/strong>&nbsp; \u5bb6\u5154\u7ecf\u773c\uff1a100%\uff0c\u91cd\u5ea6\u523a\u6fc0\uff08\u7528\u6c34\u51b2\u6d17\uff09<\/p>\n<p><strong>3.\u4e9a\u6025\u6027\u4e0e\u6162\u6027\u6bd2\u6027<sup>[18]<\/sup> <\/strong>&nbsp;\u5927\u9f20\u5438\u51652500mg\/m<sup>3<\/sup>\uff0c\u6bcf\u59296h\uff0c\u51715d\uff0c16\u53ea\u4e2d\u67098~10\u53ea\u6b7b\u4ea1\uff0c\u5c38\u89e3\u53ef\u89c1\u809d\u810f\u548c\u80ba\u810f\u635f\u4f24\u3002<\/p>\n<p>&nbsp;<\/p>\n<\/p>\n<h2 id=\"st\">\u751f\u6001\u5b66\u6570\u636e<\/h2>\n<p><p><strong>1.\u751f\u6001\u6bd2\u6027<sup>[19]<\/sup><\/strong><\/p>\n<p>LC50\uff1a1430mg\/L\uff0896h\uff09\uff08\u9ed1\u5934\u5446\u9c7c\uff09\uff1b10000~13000mg\/L\uff0896h\uff09\uff08\u8679\u9cdf\u9c7c\uff09<\/p>\n<p><strong>2.\u751f\u7269\u964d\u89e3\u6027<\/strong>&nbsp; \u6682\u65e0\u8d44\u6599<\/p>\n<p><strong>3.\u975e\u751f\u7269\u964d\u89e3\u6027<sup>[20]<\/sup> &nbsp;<\/strong>\u7a7a\u6c14\u4e2d\uff0c\u5f53\u7f9f\u57fa\u81ea\u7531\u57fa\u6d53\u5ea6\u4e3a5.00\u00d710<sup>5<\/sup>\u4e2a\/cm<sup>3<\/sup>\u65f6\uff0c\u964d\u89e3\u534a\u8870\u671f\u4e3a22h\uff08\u7406\u8bba\uff09\u3002<strong><\/strong><\/p>\n<\/p>\n<h2 id=\"fz\">\u5206\u5b50\u7ed3\u6784\u6570\u636e<\/h2>\n<p><p>1\u3001\u6469\u5c14\u6298\u5c04\u7387\uff1a19.85<\/p>\n<p>2\u3001\u6469\u5c14\u4f53\u79ef\uff08cm<sup>3<\/sup>\/mol\uff09\uff1a82.6<\/p>\n<p>3\u3001\u7b49\u5f20\u6bd4\u5bb9\uff0890.2K\uff09\uff1a186<\/p>\n<p>4\u3001\u8868\u9762\u5f20\u529b\uff08dyne\/cm\uff09\uff1a25.7<\/p>\n<p>5\u3001\u4ecb\u7535\u5e38\u6570\uff08F\/m\uff09\uff1a36.7<\/p>\n<p>6\u3001\u5076\u6781\u8ddd\uff08D\uff09\uff1a3.86\uff081D=3.33\u00d710-<sup>30<\/sup>C\u00b7m\uff09<\/p>\n<p>7\u3001\u6781\u5316\u7387\uff0810<sup>-24<\/sup>cm<sup>3<\/sup>\uff09\uff1a7.87<\/p>\n<\/p>\n<h2 id=\"js\">\u8ba1\u7b97\u5316\u5b66\u6570\u636e<\/h2>\n<p><p>1\u3001\u758f\u6c34\u53c2\u6570\u8ba1\u7b97\u53c2\u8003\u503c\uff08XlogP\uff09\uff1a-1<\/p>\n<p>2\u3001\u6c22\u952e\u4f9b\u4f53\u6570\u91cf\uff1a0<\/p>\n<p>3\u3001\u6c22\u952e\u53d7\u4f53\u6570\u91cf\uff1a1<\/p>\n<p>4\u3001\u53ef\u65cb\u8f6c\u5316\u5b66\u952e\u6570\u91cf\uff1a0<\/p>\n<p>5\u3001\u62d3\u6251\u5206\u5b50\u6781\u6027\u8868\u9762\u79ef\uff08TPSA\uff09\uff1a20.3<\/p>\n<p>6\u3001\u91cd\u539f\u5b50\u6570\u91cf\uff1a5<\/p>\n<p>7\u3001\u8868\u9762\u7535\u8377\uff1a0<\/p>\n<p>8\u3001\u590d\u6742\u5ea6\uff1a33.9<\/p>\n<p>9\u3001\u540c\u4f4d\u7d20\u539f\u5b50\u6570\u91cf\uff1a0<\/p>\n<p>10\u3001\u786e\u5b9a\u539f\u5b50\u7acb\u6784\u4e2d\u5fc3\u6570\u91cf\uff1a0<\/p>\n<p>11\u3001\u4e0d\u786e\u5b9a\u539f\u5b50\u7acb\u6784\u4e2d\u5fc3\u6570\u91cf\uff1a0<\/p>\n<p>12\u3001\u786e\u5b9a\u5316\u5b66\u952e\u7acb\u6784\u4e2d\u5fc3\u6570\u91cf\uff1a0<\/p>\n<p>13\u3001\u4e0d\u786e\u5b9a\u5316\u5b66\u952e\u7acb\u6784\u4e2d\u5fc3\u6570\u91cf\uff1a0<\/p>\n<p>14\u3001\u5171\u4ef7\u952e\u5355\u5143\u6570\u91cf\uff1a1<\/p>\n<\/p>\n<h2 id=\"xz\">\u6027\u8d28\u4e0e\u7a33\u5b9a\u6027<\/h2>\n<p><p>1.\u4e3a\u975e\u8d28\u5b50\u578b\u6781\u6027\u6eb6\u5242\uff0c\u5bf9\u591a\u79cd\u6709\u673a\u5316\u5408\u7269\u548c\u65e0\u673a\u5316\u5408\u7269\u5747\u6709\u826f\u597d\u7684\u6eb6\u89e3\u80fd\u529b\uff0c\u5728\u65e0\u78b1\u3001\u9178\u3001\u6c34\u5b58\u5728\u4e0b\uff0c\u5177\u6709\u826f\u597d\u7684\u5316\u5b66\u7a33\u5b9a\u6027\u3002<\/p>\n<p>2.\u5316\u5b66\u6027\u8d28\uff1a\u5728\u65e0\u9178\u3001\u78b1\u3001\u6c34\u5b58\u5728\u4e0b\uff0c\u5373\u4f7f\u52a0\u70ed\u5230\u6cb8\u70b9\u4e5f\u662f\u6bd4\u8f83\u7a33\u5b9a\u7684\u3002\u5728\u9178\u7684\u4f5c\u7528\u4e0b\u5206\u89e3\u6210\u7532\u9178\u548c\u4e8c\u7532\u80fa\u76d0\uff0c\u800c\u5728\u78b1\u7684\u4f5c\u7528\u4e0b\u5219\u5206\u89e3\u6210\u7532\u9178\u76d0\u548c\u4e8c\u7532\u80fa\u3002<\/p>\n<p>3.\u53d7\u7d2b\u5916\u7ebf\u4f5c\u7528\u5206\u89e3\u6210\u4e8c\u7532\u80fa\u4e0e\u7532\u919b\uff0c\u52a0\u70ed\u5230350\u2103\u5de6\u53f3\u5206\u89e3\u6210\u4e8c\u7532\u80fa\u4e0e\u4e00\u6c27\u5316\u78b3\u3002\u4e0e\u76d0\u9178\u5f62\u6210\u6bd4\u8f83\u7a33\u5b9a\u7684\u7b49\u6469\u5c14\u7684\u52a0\u5408\u7269\uff0c\u5176\u7194\u70b9\u4e3a40\u2103\uff0c\u6cb8\u70b9\u4e3a110\u2103\u3002\u4e0eSO3\u4e5f\u80fd\u5f62\u6210\u7ed3\u6676\u6027\u52a0\u5408\u7269\uff0c\u5176\u7194\u70b9\u4e3a138\u2103\uff0c\u6cb8\u70b9\u4e3a145\u2103\uff0cDMF-SO3\u53ef\u4f5c\u4e3a\u7f13\u548c\u7684\u78fa\u5316\u5242\u548c\u5316\u5242\u4f7f\u7528\u3002\u4e0ePOCl3\u3001COCl2\u3001SOCl2\u7b49\u5f62\u6210\u7684\u52a0\u5408\u7269\u53ef\u5728\u7535\u5b50\u5bc6\u5ea6\u9ad8\u7684\u82b3\u9999\u73af\u4e0a\u5f15\u5165CHO\u57fa\uff08Vilsmeier\u53cd\u5e94\uff09\u3002P2O5\u5728\u5ba4\u6e29\u4e0b\u4e0d\u6eb6\u4e8eN,N-\u4e8c\u7532\u57fa\u7532\u9170\u80fa\uff0c\u4f46\u572840\u2103\u4ee5\u4e0a\u5f62\u6210\u7a33\u5b9a\u7684\u7edc\u5408\u7269\u540e\uff0c\u5728\u5ba4\u6e29\u5373\u80fd\u6eb6\u89e3\uff0c\u800c\u4e0d\u53d1\u751f\u6c89\u6dc0\u3002\u5728\u91d1\u5c5e\u94a0\u5b58\u5728\u4e0b\u52a0\u70ed\u65f6\u53d1\u751f\u6fc0\u70c8\u53cd\u5e94\u5e76\u653e\u51fa\u6c22\u6c14\u3002\u4e0e\u4e09\u4e59\u57fa\u94dd\u57280\u2103\u4e5f\u80fd\u53d1\u751f\u6fc0\u70c8\u53cd\u5e94\u3002\u4e5f\u80fd\u4e0eGrignard\u8bd5\u5242\u53cd\u5e94\u3002\u4e0e\u9170\u6c2f\u53ca\u9178\u9150\u53d1\u751f\u53cd\u5e94\u65f6\u751f\u6210\u4e8c\u7532\u9170\u80fa\u7684\u884d\u751f\u7269\u3002<\/p>\n<p>4.\u5c5e\u4f4e\u6bd2\u7c7b\u3002\u52a8\u7269\u8bd5\u9a8c\u8bc1\u660e\uff0c\u8fde\u7eed\u6295\u7ed9\u5927\u91cf\u7684N,N-\u4e8c\u7532\u57fa\u7532\u9170\u80fa\u65f6\uff0c\u5f15\u8d77\u4f53\u91cd\u51cf\u8f7b\uff0c\u5e76\u963b\u788d\u9020\u8840\u673a\u80fd\u3002\u5bf9\u773c\u3001\u76ae\u80a4\u3001\u9ecf\u819c\u6709\u5f3a\u70c8\u7684\u523a\u6fc0\u4f5c\u7528\uff0c\u5176\u6db2\u4f53\u6216\u84b8\u6c14\u88ab\u76ae\u80a4\u5438\u6536\u540e\u8fd8\u80fd\u5f15\u8d77\u809d\u810f\u969c\u788d\u3002\u5438\u5165\u9ad8\u6d53\u5ea6\u7684\u84b8\u6c14\u80fd\u5f15\u8d77\u6025\u6027\u4e2d\u6bd2\uff0c\u4e3b\u8981\u75c7\u72b6\u4e3a\u4e25\u91cd\u523a\u6fc0\u3001\u5168\u8eab\u75c9\u631b\u3001\u75bc\u75db\u6027\u4fbf\u79d8\u548c\u6076\u5fc3\u3001\u5455\u5410\u7b49\u3002\u6162\u6027\u4e2d\u6bd2\u9664\u6709\u76ae\u80a4\u3001\u9ecf\u819c\u523a\u6fc0\u5916\uff0c\u5c1a\u6709\u6076\u5fc3\u3001\u5455\u5410\u3001\u80f8\u95f7\u3001\u5934\u75db\u3001\u5168\u8eab\u4e0d\u9002\u3001\u98df\u6b32\u51cf\u5c11\u3001\u80c3\u75db\u3001\u4fbf\u79d8\u3001\u809d\u5927\u548c\u809d\u529f\u80fd\u53d8\u5316\u3001\u5c3f\u80c6\u7d20\u539f\u548c\u5c3f\u80c6\u7d20\u4ea6\u53ef\u589e\u52a0\u3002\u4f7f\u7528\u65f6\u8981\u6c42\u5e73\u5747\u84b8\u6c14\u6d53\u5ea6\u572829.9mg\/m3\u4ee5\u4e0b\uff0c59.8mg\/m3\u65f6\u5373\u51fa\u73b0\u4e2d\u6bd2\u75c7\u72b6\uff08\u4f24\u5bb3\u4e2d\u67a2\u795e\u7ecf)\u3002\u5927\u9f20\u548c\u5c0f\u9f20\u7684\u7ecf\u53e3\u6bd2\u6027LD50\u4e3a3000~7000mg\/kg\u3002\u55c5\u89c9\u9608\u6d53\u5ea60.14mg\/m3\uff0cTJ 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src=\"https:\/\/www.51dmea.cn\/wp-content\/uploads\/2024\/04\/201009131410573534.gif\" width=\"231\" height=\"47\" alt=\"\" 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